In-Situ Transmission Electron Microscopy Experiments - Design and Practice
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| Verlag | Wiley-VCH |
| Auflage | 2023 |
| Seiten | 384 |
| Format | 21,7 x 2,4 x 26,7 cm |
| Gewicht | 898 g |
| Artikeltyp | Englisches Buch |
| ISBN-10 | 3527347984 |
| EAN | 9783527347988 |
| Bestell-Nr | 52734798A |
A comprehensive guide to planning and performing in situ TEM measurements that explains the basic principles and current approaches for in situ/operando measurements of material morphology, structure and chemical changes under different kinds of stimuli. Written for practitioners, it addresses experimental limitations and shows how to overcome them, explains how work with and enhance commercially available equipment, and discusses future perspectives in the field. Throughout, the reader will find practical advice and hands-on knowledge from the author's life-long efforts in extending the boundaries of this novel technology.
Inhaltsverzeichnis:
IN-SITU TEM
General Scope of the Book and Review of the Chapters
Why in-situ TEM?
TEM Overview
TEM/STEM-Based Characterization Techniques
Other Techniques
Introduction to Different Stimuli Used for In situ TEM
EXPERIMENT DESIGN PHILOSOPHY
General Aspects
Choice of Technique and the Microscope
TEM Holder Design and Selection
Specimen Design and Preparation
Guidelines for Experimental Setup
Practical Example of Designing In-situ TEM Experiments
Applications to Quantitative Data
IN-SITU HEATING
History
Currently Available Heating Holders
Experimental Considerations
Select Applications
Limiations and Possibilities
IN SITU CRYO-TEM
Historical Perspective
Specimen Holder Design and Function
Specimen Design and Preparation
Practical Aspects of Performing Cryogenic Cooling
Some Noteworthy Applications
DESIGNING LIQUID AND GAS CELL HOLDERS
Historical Perspective
Design Philosophy
W indows
Microfabricated Window-Cell (Microchips)
Examples of Modified Window Holders
IN SITU SOLID-LIQUID INTERACTIONS
Historical Perspective
Holder Design and Selection
Specimen Design and Preparation
Data Acquisition
Practical Challenges
Select Examples of Applications
IN-SITU GAS-SOLID INTERACTIONS
Historical Perspective
Current Strategies
Gas Manifold Design and Construction
Practical Aspects of Performi Experiment in Gas Environments
Select Examples of Applications
Review of Benefits and Limitations
MULTIMODAL AND CORRELATIVE MICROSCOPY
Multimodal TEM
Correlative Approaches
DATA PROCESSING AND MACHINE LEARNING
History of Image Simulation and Processing
Current Status
Data Management
Data Processing and Machine Learning (ML)
Select Applications
Future Needs
Limitations
FUTURE VISION
Historical Aspects
Current Status
Technical Challenges
Developing Relevant St rategies
